| 李顺发1,邓雨冰1,胡醇1,王良俊2,张清1.葡聚糖接枝大豆分离蛋白Pickering乳液的
制备与性质研究[J].中国油脂,2025,50(12):.[LI Shunfa1, DENG Yubing1, HU Chun1, WANG Liangjun2, ZHANG Qing1.Preparation and properties of dextran grafted soybean protein isolate-based Pickering emulsions[J].China Oils and Fats,2025,50(12):.] |
| 葡聚糖接枝大豆分离蛋白Pickering乳液的
制备与性质研究 |
| Preparation and properties of dextran grafted soybean protein isolate-based Pickering emulsions |
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| DOI:10.19902/j.cnki.zgyz.1003-7969.240727 |
| 中文关键词: Pickering乳液 乳液稳定性 乳液性质 大豆分离蛋白 大豆分离蛋白-葡聚糖共轭物 |
| 英文关键词:Pickering emulsions emulsion stability emulsion property soybean protein isolate soybean protein isolate-dextran conjugate |
| 基金项目:四川天府新区眉山管委员会科技合作项目(2322339004);雅安市-四川农业大学市校合作项目(23ZDYF0003) |
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| Author Name | Affiliation | | LI Shunfa1, DENG Yubing1, HU Chun1, WANG Liangjun2, ZHANG Qing1 | 1.College of Food Science, Sichuan Agricultural University, Ya′an 625014, Sichuan, China 2.Rural
Revitalization and Development Service Center of Meishan Tianfu New District, Meishan 620000,
Sichuan, China |
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| 中文摘要: |
| 旨在为脂溶性生物活性物质的包埋递送提供参考,以大豆分离蛋白(SPI)-葡聚糖共轭物(SDC)为乳化剂和稳定剂,采用两步法运用高压微射流制备Pickering乳液(SDC-PEs),通过单因素实验研究了均质压力、均质次数、SDC添加量对乳液粒径和多分散指数(PDI)的影响,并采用响应面实验对SDC-PEs的制备条件进行了优化。另外,对最佳工艺条件下制备的SDC-PEs性质进行了分析。结果表明:SDC-PEs的最佳制备工艺条件为均质压力140 MPa 、均质次数6次、SDC添加量2.13%、油相体积分数10%,在此条件下SDC-PEs的平均粒径为210.33 nm,PDI小于0.20;SDC-PEs表现出良好的pH稳定性、抗离子强度稳定性、温度稳定性和储存稳定性,且优于以SPI稳定的Pickering乳液(SPI-PEs)。综上,通过添加SDC可以制备出稳定性良好的Pickering乳液。 |
| 英文摘要: |
| To provide a reference for the encapsulation and delivery of lipophilic bioactive substances, Pickering emulsions (SDC-PEs)was prepared by using a two-step method of high-pressure microfluidization process with soybean protein isolate(SPI)-dextran conjugate(SDC) as emulsifier and stabilizer. Single-factor experiments were conducted to investigate the effects of homogenization pressure, homogenization times, and SDC dosage on emulsion particle size and polydispersity index (PDI). The preparation conditions of SDC-PEs were further optimized using response surface methodology. Additionally, the properties of SDC-PEs prepared under the optimal conditions were analyzed. The results showed that the optimal preparation parameters of SDC-PEs were as follows: homogenization pressure 140 MPa, homogenization times 6, SDC dosage 2.13%, and volume fraction of oil phase 10%. Under these conditions, SDC-PEs exhibited an average particle size of 210.33 nm with a PDI below 020. The SDC-PEs showed excellent stability against pH, ionic strength, temperature, and storage, outperforming SPI-stabilized Pickering emulsions (SPI-PEs). In conclusion, Pickering emulsions with good stability can be prepared by adding SDC. |
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