| 俞 晔,金青哲,王 玥，等.HPLC-FLD快速测定大豆中的多环芳烃[J].中国油脂,2013,38(7):.[YU Ye,JIN Qingzhe,WANG Yue,etc.Rapid assay of polycyclic aromatic hydrocarbons in soybean by HPLC-FLD[J].China Oils and Fats,2013,38(7):.] |
| HPLC-FLD快速测定大豆中的多环芳烃 |
| Rapid assay of polycyclic aromatic hydrocarbons in soybean by HPLC-FLD |
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| DOI： |
| 中文关键词: HPLC-FLD 大豆 多环芳烃 |
| 英文关键词:HPLC-FLD soybean polycyclic aromatic hydrocarbons |
| 基金项目: |
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| 摘要点击次数: 1569 |
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| 中文摘要: |
| 建立了大豆中多环芳烃的快速检测方法。采用乙腈-四氢呋喃（1+1）提取大豆中的多环芳烃，并用高效液相色谱-荧光光谱（HPLC-FLD）法测定多环芳烃含量。方法检出限和定量限分别为0.07～0.61 μg/kg和0.27～2.04 μg/kg，线性范围为2～200 μg/kg，回收率在81.7%～96.5%之间，相对标准偏差在 2.10%～10.44%之间。 |
| 英文摘要: |
| A rapid method for detecting polycyclic aromatic hydrocarbons (PAHs) in soybean was developed. After the soybean was treated with acetonitrile-tetrahydrofuran (1∶1), the PAHs contents were determined by HPLC-FLD. The detection limit and the limit of quantification of the method were 0.07-0.61 μg/kg and 0.27-2.04 μg/kg, respectively. For the twelve PAHs, the method had a good linear range, which was 2-200 μg/kg. The recovery rate ranged from 81.7% to 96.5% and the relative standard deviation was in the range of 2.10%-10.44%. |
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