刘德阳,孔祥珍,华欲飞,等.氯化钙诱导大豆分离蛋白冷凝胶相图与流变性质研究[J].中国油脂,2015,40(8):.[LIU Deyang,KONG Xiangzhen,HUA Yufei,etc.Rheological properties and phase diagram of CaCl2-induced soy protein isolate cold-set gel[J].China Oils and Fats,2015,40(8):.]
氯化钙诱导大豆分离蛋白冷凝胶相图与流变性质研究
Rheological properties and phase diagram of CaCl2-induced soy protein isolate cold-set gel
  
DOI:
中文关键词:  大豆分离蛋白  冷凝胶  CaCl2  相图  流变性质
英文关键词:soy protein isolate  cold-set gel  CaCl2  phase diagram  rheological property
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刘德阳  
孔祥珍  
华欲飞,等  
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中文摘要:
      主要研究了CaCl2诱导大豆分离蛋白冷凝胶在不同预加热温度、蛋白质含量和盐浓度下的相图、持水性与流变性质。结果表明:随着预加热温度的升高(75~95℃),诱导大豆分离蛋白冷凝胶形成所需要的CaCl2浓度降低,且相同条件下,蛋白质含量越高,冷凝胶越易形成;冷凝胶持水性与蛋白质含量成正比,与CaCl2浓度成反比,而在85℃预加热温度下冷凝胶持水性最高,75℃预加热温度条件下冷凝胶持水性最低;随着蛋白质含量、预加热温度和CaCl2浓度增加,冷凝胶的凝胶强度和屈服应力逐渐增加;冷凝胶的线性黏弹性区域(LVE)在15 mmol/L CaCl2浓度下随蛋白质含量增加而增加,但在10 mmol/L CaCl2浓度下呈现出相反的变化趋势;15 mmol/L CaCl2诱导冷凝胶在一定应变下会发生流动现象,而10 mmol/L CaCl2诱导冷凝胶没有流动现象,表明两种CaCl2浓度下形成的冷凝胶结构有很大差异。
英文摘要:
      The phase diagram, water holding capacity(WHC) and rheological properties of CaCl2-induced soy protein isolate cold-set gel under the conditions of different preheating temperatures, protein contents and salt concentrations were studied. The results showed that with the increase of preheating temperature(from 75℃ to 95℃), CaCl2 concentration which was needed to form soy protein isolate cold-set gel decreased, and under the same condition, the higher the protein content, the easier the formation of cold-set gel; WHC of cold-set gel had a positive correlation with protein content and negative correlation with CaCl2 concentration. Under the condition of preheating temperature 85℃,the WHC of cold-set gel was the highest, while it was the lowest under the condition of preheating temperature 75℃; with the increases of protein content,preheating temperature and CaCl2 concentration, the gel strength and yield stress of the cold-set gel improved.The linear viscoelastic region of cold-set gel induced by 15 mmol/L CaCl2 was positively correlated with protein content,while it showed opposite trends with the increase of protein content when the cold-set gel was induced by 10 mmol/L CaCl2. The cold-set gel induced by 15 mmol/L CaCl2 could flow with certain strain, while the cold-set gel induced by 10 mmol/L CaCl2 couldn’t flow under the same condition, which indicated that the structures of cold-set gels induced by 10 mmol/L CaCl2 and 15 mmol/L CaClv were very different.
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