芝麻油浓缩磷脂提取工艺条件的研究
Extraction of phospholipids concentrate from sesame oil sediment
  
DOI:
中文关键词:  芝麻油脚  浓缩磷脂  正己烷萃取  水化浓缩  絮凝分离
英文关键词:sesame oil sediment  phospholipids concentrate  n-hexane extraction  hydration concentration  flocculation separation
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Author NameAffiliation
LIU Yulan  
PENG Minghui  
,JI Huairui  
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中文摘要:
      以水代法和机榨法制取的芝麻毛油静置沉淀后的底部沉淀物(即芝麻油脚)为原料,利用正己烷萃取除杂、水化浓缩及絮凝分离的方法从中提取芝麻油浓缩磷脂,并对水化浓缩和絮凝分离的工艺条件进行了研究。结果表明:正己烷萃取除杂(条件为料液比1∶8、时间6 h、温度25℃)后芝麻油脚中固体不溶性杂质含量从21.25%降低至0.04%;水化浓缩的最佳条件为水与萃取除杂油脚质量比4.5∶1、水化时间40 min、水化温度85℃,水化浓缩后丙酮不溶物含量从3.41%提高至45.87%;絮凝分离的最佳条件为预热温度40℃、反应温度90℃、NaCl添加量3%、反应时间20 min,所得浓缩磷脂的丙酮不溶物含量为56.82%。
英文摘要:
      The crude sesame oil produced by aqueous extraction or pressing was placed,and the deposit (sesame oil sediment) was used as raw material,and phospholipids concentrate was extracted by impurity removal with n-hexane,hydration concentration and flocculation separation. The optimal extraction processes of hydration concentration and flocculation separation were researched. The results showed that the content of insoluble solid impurities decreased from 21.25% to 0.04% by impurity removal with n-hexane under the conditions of ratio of n-hexane to sesame oil sediment 8∶]1,time 6 h and temperature 25℃. The optimal conditions of hydration concentration were as follows:hydration temperature 85℃,mass ratio of water to sesame oil sediment after impurity removal 4.5∶1,hydration time 40 min;under these conditions,the content of acetone insoluble matter increased from 3.41% to 45.87%. The optimal conditions of flocculation separation were as follows:preheating temperature 40℃,reaction temperature 90℃,sodium chloride dosage 3%,reaction time 20 min;under these conditions,the acetone insoluble matter content of phospholipid concentrate obtained was 56.82%.
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