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Ultrasound-assisted extraction and GC-MS analysis of Xinjiang pomegranate seed oil |
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KeyWord:Xinjiang pomegranate seed oil ultrasound-assist extraction process optimization GC-MS |
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Abstract: |
With Xinjiang pomegranate seed as raw material,pomegranate seed oil was extracted by ultrasound-assisted solvent method. On the basis of single factor experiment,the extraction conditions were optimized by orthogonal experiment. The results showed that the optimal extraction conditions were obtained as follows:with petroleum ether (60-90℃) as extraction solvent, particle size of pomegranate seed powder 60 meshes, solid-liquid ratio 1∶10,ultrasonic power 240 W,ultrasonic treatment time 50 min and ultrasonic treatment temperature 45℃. Under these conditions,the yield of pomegranate seed oil was 15.09%. The analysis results of GC-MS indicated that the main fatty acids of pomegranate seed oil were as follows:palmitic acid 6.24%,linoleic acid 14.64%,oleic acid 11.11%,stearic acid 3.97%,punicic acid 43.46%,9,12,15-octadecatrienoic acid 11.31% and 6,9,12-octadecatrienoic acid 9.28%. |
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