Preparation of fatty acid monoglyceride by non-precious metal salts catalyzed ring-opening reaction
  
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KeyWord:glycidyl laurate  ring-opening reaction  glycerol monolaurate  preparation
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CAO Didi, XUE Yuanqiang, FAN Qiaoying,etc  
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Abstract:
      High-purity glycerol monolaurate was obtained by hydrolytic ring-opening of glycidyl laurate and freezing crystallization, which catalyzed by non-precious metal inorganic salts. The preparation conditions of glycerol monolaurate were optimized as follows: with acetonitrile as solvent, and CuCl2 as catalyst, dosage of CuCl2 8%(based on the mole of glycerol monolaurate), reaction time 24 h. Furthermore, the method was applied to prepare glycerol monopalmitate and glycerol monostearate, and these products were characterized by FT-IR and ESI-MS, which confirmed the validity of the preparation method.
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