UPLC-PDA-MS鉴定经大孔树脂纯化美藤果壳酚类物质
Identification of phenolic compounds from Sacha Inchi shells purified by macroporous resin using UPLC-PDA-MS
  
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中文关键词:  美藤果壳酚类物质  预制薄层层析法  UPLC-PDA-MS  结构鉴定
英文关键词:phenolic compounds from Sacha Inchi shells  preparative thin layer chromatography  UPLC-PDA-MS  structure identification
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YANG Wan, DUAN Jiahui, ZHAO Chenwei,etc  
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中文摘要:
      以经大孔树脂纯化的美藤果壳酚类物质为原料,用预制硅胶板薄层层析法将其粗分为4个条带,富集各个条带中的物质后使用UPLC-PDA-MS检测,确定其中的酚类物质为:1号条带中有香草酸己糖苷,1,2-芥子酰阿魏酸酰龙胆二糖(待定),矢车菊素3-(6″-阿魏酰槐糖苷)-5-葡糖苷,锦葵花色素3-葡萄糖苷,锦葵花色素3-葡萄糖苷二倍体;2号条带中有香草酸己糖苷,香草酸己糖苷三倍体以及香草酸己糖苷二倍体;3号条带中有对羟基苯甲酸,羟基苯甲酸己糖苷,对香豆酸己糖苷以及对香豆酸四倍体;4号条带中有对羟基苯甲酸以及对香豆酸。
英文摘要:
      The phenolic compounds from Sacha Inchi shells purified by macroporous resin were divided into four bands by preparative thin layer chromatography. Then UPLC-PDA-MS was used to analyze the compounds in every band after enrichment. The structures of phenolic compounds were identified as follows: vanillic acid hexoside, 1,2-disinapoyl-feruloyl-gentiobiose (undecided), cyanidin 3-(6″-feruloylsophoroside)-5-glucoside, malvidin 3-glucoside and malvidin 3-glucoside dimer in band 1; vanillic acid hexoside, vanillic acid hexoside trimer and vanillic acid hexoside dimer in band 2; p-hydroxybenzoic acid, hydroxybenzoic acid hexoside, p-coumaroyl hexose and p-coumaric acid tetramer in band 3; p-hydroxybenzoic acid and p-coumaric acid in band 4.
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