Determination of procymidone and flusilazole pesticides in vegetable oil by GC-MS
  
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KeyWord:vegetable oil  procymidone  flusilazole  pesticide
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YANG Tianqing, HAN Juan, GONG Shan,etc  
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Abstract:
      Using QuEChERS rapid purification column to pretreat sample, the procymidone and flusilazole pesticides residues in vegetable oil were determined by GC-MS. The results showed that the recoveries of procymidone and flusilazole were 85.0%-96.0% and 88.3%-94.1%, respectively; the intra-laboratory variation coefficients of procymidone and flusilazole were 1.5%-8.9% and 2.1%-68%, respectively; the detection limits of procymidone and flusilazole were 0.007 5 mg/kg and 0.022 5 mg/kg, respectively. The method had the advantages of simple pretreatment, high sensitivity and good reproducibility.
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