Extraction of lipid minor compounds from rapeseed cake by subcritical r134a-butane
  
DOI:10.12166/j.zgyz.1003-7969/2019.11.021
KeyWord:rapeseed cake  subcritical fluid extraction  r134a-butane  minor compound
FundProject:国家重点研发计划项目(2017YFD0400402);国家自然科学基金(31501409)
Author NameAffiliation
GUO Tingting1,2,3, WAN Chuyun1,2,3, HUANG Fenghong1,3 1.Oil Crops Research Institute of the Chinese Academy of Agricultural Sciences, Wuhan 430062, China
2.Oil Crops and Lipids Process Technology National & Local Joint Engineering Laboratory, Wuhan 430062, China
3.Key Laboratory of Oilseeds Processing, Ministry of Agriculture, Wuhan 430062, China 
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Abstract:
      The extraction amounts of Canolol, tocopherol and phytosterol were used as the indexes and the rapeseed cake was as material, the effects of mass ratio of r134a to butane were studied. The optimal extraction conditions were obtained by orthogonal experiment as follows: mass ratio of r134a to butane 6∶ 3, extraction temperature 45 ℃ and extraction time 30 min. Under these conditions, the extraction amounts of Canolol, total tocopherol and total phytosterol were 2.43, 9.71, 89.17 mg/100 g, respectively.
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