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Process optimization of enrichment of unsaturated fatty acids in hump oil by urea adduction |
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DOI:10.12166/j.zgyz.1003-7969/2020.04.003 |
KeyWord:hump oil urea adduction unsaturated fatty acid enrichment |
FundProject:内蒙古自治区科技创新引导项目(KCMS2018048);内蒙古自治区科技重大项目;内蒙古自然科学基金项目(2018BS03017);双一流学科创新团队建设(NDSC2018-14);高层次人才引进科研启动项目(NDYB2017-28) |
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Abstract: |
With mixed fatty acid of refined hump oil (SFA 54.024 3%, MUFA 34.645 7%, PUFA 4645 3%) as raw material, on the basis of single factor experiment, the enrichment process of unsaturated fatty acids in hump oil by urea adduction was optimized by response surface methodology. The results showed that the optimal enrichment process conditions were obtained as follows: ratio of urea mass to 95% ethanol volume 3∶ 8, mass ratio of urea to mixed fatty acid 3.315∶ 1, adduction temperature-2.37 ℃, and adduction time 1813 h. Under these conditions, the iodine value of the product was 125.73 gI/100 g, and the contents of SFA, MUFA and PUFA in the product were 7.802 5%, 58.175 6% and 17322 2% respectively. The product after urea adduction was viscous liquid with light yellow, and the content of unsaturated fatty acid was about 75%. |
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