Rapid determination of oryzanol in rice bran oil by near-infrared spectroscopy
  
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KeyWord:near-infrared spectroscopy  oryzanol  quantitative analysis model  rice bran oil
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Author NameAffiliation
PENG Zhibing1,XIONG Xiaohui1,YU Lu2,ZHANG Chen1,HU Chun1 1.Food Inspection and Testing Research Institute of Jiangxi General Institute of Testing and Certification, Nanchang 330046, China
2.Beijing Branch of PerkinElmer Limited Company, Beijing 100015,China 
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Abstract:
      In order to determine the oryzanol content in rice bran oil with a simple, rapid and accurate manner, a quantitative analysis model of near-infrared spectroscopy combined with partial least squares method for the determination of oryzanol content in rice bran oil was established by using the high performance liquid chromatography method of LS/T 6121.2-2017 as the reference method. The results showed that the coefficient of deterination of quantitative analysis model established was 99.81%, the standard deviation of prediction was 0.028 49%, and the standard deviation of cross validation was 0.031 13%. The total of 99 samples were used to the external independent verification of the quantitative analysis model, and the coefficient of deterination of prediction was 99.81%, the standard deviation of prediction was 0.030 90%, the absolute error was in the range of -0.081%-0.057%, relative error was in the range of -11.86%-9.84%. The established quantitative analysis model has good prediction effect and high accuracy, and can be used for the determination of oryzanol content in rice bran oil.
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