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Optimization of decolorization process of rosemary fat-soluble extract by response surface methodology |
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DOI: |
KeyWord:rosemary fat-soluble extract decolorization corn oil carnosic acid carnosic phenol |
FundProject:湖南省自然科学基金项目(2022JJ50212);邵阳学院研究生科研创新项目(CX2021SY072) |
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Abstract: |
In order to provide a reference for the application of rosemary fat-soluble extract in the preservation of edible oil, the rosemary fat-soluble extract (which can be used as an antioxidant) extracted by corn oil was decolorized. With the decolorization rate as the index, the decolorization process conditions were optimized by single factor experiment and response surface methodology, and the content of fat-soluble antioxidant components (carnosic acid and carnosic phenol) in rosemary fat-soluble extract before and after decolorization was determined by high performance liquid chromatography. The results showed that activated carbon had the best decolorization effect on rosemary fat-soluble extract compared with activated clay and compound decolorant of activated clay and activated carbon (mass ratio 1∶ 1,1∶ 2,2∶ 1). The optimal decolorization process conditions were as follows: activated carbon dosage2.1%, decolorization temperature 50 ℃, decolorization time 59 min. Under the optimal conditions, the decolorization rate was (75.02±0.37)%. The antioxidant content before and after decolorization in rosemary fat-soluble extract was 4.065 5% and 3.883 6%, respectively. In summary, the decolorization effect of rosemary fat-soluble extract under optimized conditions was better, and the decolorization had little effect on the content of fat-soluble antioxidant components. |
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